3-(Allyloxy)benzoyl chloride

Base Information

Chemical Name:3-(Allyloxy)benzoyl chloride
CAS No.:83230-73-3
Molecular Formula:C10H9 Cl O2
Molecular Weight:196.63026
Hs Code.:2918990090
DSSTox Substance ID:DTXSID90524982
Wikidata:Q82392261
Mol file:83230-73-3.mol

Synonyms:83230-73-3;3-(Allyloxy)benzoyl chloride;SCHEMBL5729029;DTXSID90524982;AKOS030220497;3-(allyloxy)-1-benzenecarbonyl chloride;3-[(Prop-2-en-1-yl)oxy]benzoyl chloride

Suppliers and Price of 3-(Allyloxy)benzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-(Allyloxy)benzoyl chloride

Chemical Property:

PSA：26.30000
LogP:2.63040
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:196.0291072
Heavy Atom Count:13
Complexity:191

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCOC1=CC=CC(=C1)C(=O)Cl

Technology Process of 3-(Allyloxy)benzoyl chloride

There total 2 articles about 3-(Allyloxy)benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103203-83-4
3-(allyloxy)benzoic acid

: 83230-73-3
3-allyloxy-benzoyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1002/jhet.5570450222

Reference yield:

: 79250-46-7
methyl 3-(prop-2-enyloxy)benzoate

: 83230-73-3
3-allyloxy-benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; potassium hydroxide; In methanol; dichloromethane;
DOI:10.1039/c4cc00029c