C₁₂H₁₇N₃O

Base Information

• Chemical Name: C₁₂H₁₇N₃O
• CAS No.: 86452-55-3
• Molecular Formula: C₁₂H₁₇N₃O
• Molecular Weight: 219.286
• Mol file: 86452-55-3.mol

Synonyms:C₁₂H₁₇N₃O

Chemical Property of C₁₂H₁₇N₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₂H₁₇N₃O

There total 3 articles about C₁₂H₁₇N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

diethylamine (109-89-7) → C12H17N3O (86452-55-3)

Guidance literature:

In water; at 20 ℃; for 0.166667h;

DOI:10.1016/j.dyepig.2013.10.022

Reference yield:

p-aminobenzophenone (99-92-3) + diethylamine (109-89-7) → 1-(p-acetophenyl)-3,3-diethyl-1-triazene (86452-55-3)

Guidance literature:

With hydrogenchloride; potassium carbonate; sodium nitrite; Multistep reaction; 1) H₂O, 0 degC, 30 min;

DOI:10.1021/jo00171a050

Reference yield:

p-aminobenzophenone (99-92-3) + diethylamine (109-89-7) → C12H17N3O (86452-55-3)

Guidance literature:

With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.) H₂O, 10 degC;

DOI:10.1055/s-1983-30306

upstream raw materials:

p-aminobenzophenone

diethylamine

Downstream raw materials:

C₁₉H₂₃ClN₄O₂

C₁₂H₁₉N₃O

4-Iodoacetophenone

benzene

Refernces

• 1、 Satyamurthy, Nagichettiar,Barrio, Jorge R.. "Cation Exchange Resin (Hydrogen Form) Assisted Decomposition of 1-Aryl-3,3-dialkyltriazenes. A Mild and Efficient Method for the Synthesis of Aryl Iodides". . p. 4394 - 4396. Retrieved 2007/10/02.
• 2、 Ku, Hao,Barrio, Jorge R.. "Convenient Synthesis of Aryl Halides from Arylamines via Treatment of 1-Aryl-3,3-dialkyltriazenes with Trimethylsilyl Halides". . p. 5239 - 5241. Retrieved 2007/10/02.