2,2-Dichloro-1-(4,5-dihydro-3-furanyl)-ethanone

Base Information

Chemical Name:2,2-Dichloro-1-(4,5-dihydro-3-furanyl)-ethanone
CAS No.:83124-81-6
Molecular Formula:C₆H₆Cl₂O₂
Molecular Weight:181.018
Hs Code.:2932190090
DSSTox Substance ID:DTXSID80435250
Nikkaji Number:J3.029.254E
Wikidata:Q82250049
Mol file:83124-81-6.mol

Synonyms:83124-81-6;2,2-DICHLORO-1-(4,5-DIHYDRO-3-FURANYL)-ETHANONE;SCHEMBL6544924;DTXSID80435250;3-(Dichloroacetyl)-4,5-dihydrofuran

Suppliers and Price of 2,2-Dichloro-1-(4,5-dihydro-3-furanyl)-ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,2-Dichloro-1-(4,5-dihydro-3-furanyl)-ethanone

Chemical Property:

PSA：26.30000
LogP:1.66340
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:179.9744848
Heavy Atom Count:10
Complexity:175

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC=C1C(=O)C(Cl)Cl

Technology Process of 2,2-Dichloro-1-(4,5-dihydro-3-furanyl)-ethanone

There total 3 articles about 2,2-Dichloro-1-(4,5-dihydro-3-furanyl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 79-36-7
dichloroacethyl chloride

: 83124-81-6
3-Dichloracetyl-4,5-dihydrofuran

Guidance literature:: With pyridine; at 0 - 40 ℃; for 3h; Ionic liquid;
DOI:10.1016/j.tetlet.2011.10.163

Reference yield:

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 79-36-7
dichloroacethyl chloride

: 83124-81-6
3-Dichloracetyl-4,5-dihydrofuran

: 83124-73-6
2-Chlor-3-dichloracetyl-tetrahydrofuran

Guidance literature:: at 0 ℃; for 17h;

Reference yield:

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 79-36-7
dichloroacethyl chloride

: 64-17-5
ethanol

: 83124-81-6
3-Dichloracetyl-4,5-dihydrofuran

: 83125-04-6
2-Ethoxy-3-dichloracetyltetrahydrofuran

Guidance literature:: With triethylamine; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) 0 deg C, 17 h, 2) 0 deg C;