(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:26295-42-1
Molecular Formula:C₂₂H₂₅N₃O₉
Molecular Weight:475.455
Hs Code.:

Synonyms:(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 24 articles about (2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 536-74-3
phenylacetylene

: 13992-25-1
1-azido-1-deoxy-β-D-glucopyranoside tetraacetate

: 26295-42-1,26295-46-5
1’-(4-phenyl-[1,2,3]-triazol-1-yl)-2’,3’,4’,6’-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: With [(PPh₃)₂Cu(μ-2,2'-thiodiacetato)Cu(PPh₃)₂]*6H₂O; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1039/c7dt02346d

Reference yield: 95.0%

: 637-44-5
phenylpropyolic acid

: 13992-25-1
1-azido-1-deoxy-β-D-glucopyranoside tetraacetate

: 26295-42-1,26295-46-5
1’-(4-phenyl-[1,2,3]-triazol-1-yl)-2’,3’,4’,6’-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: With copper(l) iodide; potassium carbonate; at 60 ℃; for 0.833333h;

Reference yield: 95.0%

: 2280-44-6
D-Glucose

: 108-24-7
acetic anhydride

: 536-74-3
phenylacetylene

: 26295-42-1,26295-46-5
1’-(4-phenyl-[1,2,3]-triazol-1-yl)-2’,3’,4’,6’-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: D-Glucose; acetic anhydride; With iodine; at 20 ℃;

With hydrogen bromide; In dichloromethane; acetic acid; at 20 ℃; for 1h;

phenylacetylene; With sodium azide; sodium hydrogencarbonate; sodium L-ascorbate; tetra(n-butyl)ammonium hydrogensulfate; copper(II) sulfate; In ethanol; chloroform; water; at 20 ℃; for 16h;
DOI:10.1016/j.tetlet.2005.01.175