C₁₄H₁₆O₂

Base Information

Chemical Name:C₁₄H₁₆O₂
CAS No.:1453112-06-5
Molecular Formula:C₁₄H₁₆O₂
Molecular Weight:216.28
Hs Code.:

C<sub>14</sub>H<sub>16</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₆O₂

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Chemical Property of C₁₄H₁₆O₂

Chemical Property:

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Technology Process of C₁₄H₁₆O₂

There total 7 articles about C₁₄H₁₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 95127-17-6
methyl 2-benzyl-3-(furan-2-yl)propanoate

: 1453112-06-5
C₁₄H₁₆O₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/ol402163u

Reference yield:

: 100-39-0
benzyl bromide

: 1453112-06-5
C₁₄H₁₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

1.2: 15 h / 60 °C

2.1: sodium tetrahydroborate / ethanol / 5 h / -78 °C

3.1: triethylamine / dichloromethane / 15 h / 0 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 15 h / 20 °C

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 5 h

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ol402163u

Reference yield:

: 615-06-5
3-furan-2-yl-3-oxo-propionic acid methyl ester

: 1453112-06-5
C₁₄H₁₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

1.2: 15 h / 60 °C

2.1: sodium tetrahydroborate / ethanol / 5 h / -78 °C

3.1: triethylamine / dichloromethane / 15 h / 0 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 15 h / 20 °C

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 5 h

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ol402163u