N-methoxy-N-methyl-3-phenylbutanamide

Base Information

Chemical Name:N-methoxy-N-methyl-3-phenylbutanamide
CAS No.:214759-91-8
Molecular Formula:C₁₂H₁₇NO₂
Molecular Weight:207.272
Hs Code.:

Synonyms:N-methoxy-N-methyl-3-phenylbutanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methoxy-N-methyl-3-phenylbutanamide

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Technology Process of N-methoxy-N-methyl-3-phenylbutanamide

There total 15 articles about N-methoxy-N-methyl-3-phenylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 4593-90-2,772-17-8
3-phenylbutyric acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 214759-91-8
N-methoxy-N-methyl-3-phenylbutanamide

Guidance literature:: 3-phenylbutyric acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 0.75h;

N,O-dimethylhydroxylamine*hydrochloride; In dichloromethane; for 24h;
DOI:10.1002/ejoc.201300392

Reference yield: 68.0%

: 1-(2,3,4,5,6-pentamethylphenyl)-3-phenylbutan-1-one

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 214759-91-8
N-methoxy-N-methyl-3-phenylbutanamide

Guidance literature:: 1-(2,3,4,5,6-pentamethylphenyl)-3-phenylbutan-1-one; With bromine; In dichloromethane; at -17 ℃; for 0.25h;

N,O-dimethylhydroxylamine*hydrochloride; With triethylamine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1002/cssc.201900990

Reference yield:

: 141868-93-1
(Z)-N-methoxy-N-methyl-3-phenylbut-2-enamide

: 214759-91-8
(R)-N-methoxy-N-methyl-3-phenylbutanamide

: (S)-N-methoxy-N-methyl-3-phenylbutanamide

Guidance literature:: (Z)-N-methoxy-N-methyl-3-phenylbut-2-enamide; With tert-Amyl alcohol; C₄₀H₄₅N₂O⁽¹⁺⁾*BF₄^(1-); copper(l) chloride; lithium tert-butoxide; In N,N-dimethyl acetamide; at 20 ℃; for 0.0833333h; Inert atmosphere; Sealed tube;

With diethoxymethylane; In N,N-dimethyl acetamide; at 25 ℃; for 15h; Overall yield = 59 percent; Overall yield = 19 mg; enantioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.3762/bjoc.16.50