[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

Base Information

Chemical Name:[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄
CAS No.:83561-95-9
Molecular Formula:C₂₄H₂₀B*C₄₃H₄₂NiP₃S₃
Molecular Weight:1125.85
Hs Code.:

[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S<sub>2</sub>CSMe)]BPh<sub>4</sub>

Synonyms:[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

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Chemical Property of [(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

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Technology Process of [(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

There total 2 articles about [(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 421-20-5
Methyl fluorosulfonate

: 83562-00-9
(CH₃C(CH₂P(C₆H₅)2)3)Ni(S₂CS)

: 143-66-8
sodium tetraphenyl borate

: 83561-95-9
[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

Guidance literature:: In ethanol; dichloromethane; MeSO3F was pipetted into a soln. of Ni-complex in CH2Cl2, NaBPh4 was added in EtOH; evapd., washed with EtOH, light petroleum, dried in a stream of N2; elem. anal.;

Reference yield:

: 421-20-5
Methyl fluorosulfonate

: 83562-00-9
[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CS)]

: 143-66-8
sodium tetraphenyl borate

: 83561-95-9
[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

Guidance literature:: In dichloromethane; complex in CH2Cl2 treated with CH3OSO2F, NaB(C6H5)4/EtOH added;

Reference yield: 90.0%

: 83561-95-9
[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

: 60294-99-7
(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

Guidance literature:: With NaBH₄; In ethanol; acetone; (N2); soln. of NaBH4 in EtOH added dropwise to Ni complex suspn. in acetone; EtOH added; elem. anal.;