1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

Base Information

Chemical Name:1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol
CAS No.:943860-54-6
Molecular Formula:C₃₄H₄₇N₃O₇SSi
Molecular Weight:669.915
Hs Code.:

Synonyms:1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

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Chemical Property of 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

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Technology Process of 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

There total 2 articles about 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 943860-58-0
1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

: 124-63-0
methanesulfonyl chloride

: 943860-54-6
1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1055/s-2007-966022

Reference yield:

: 881895-05-2
2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

: 943860-54-6
1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / DMAP / pyridine / 20 °C

2: 97 percent / pyridine / 3 h / 20 °C

With pyridine; dmap; In pyridine;
DOI:10.1055/s-2007-966022

Reference yield:

: 943860-54-6
1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

: 945927-76-4
C₃₈H₅₃NO₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Et₃N; H₂ / Pd/C / tetrahydrofuran / 20 °C / 750.08 Torr

2: 98 percent / Et₃N / CH₂Cl₂ / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2007-966022