1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

Base Information

• Chemical Name: 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol
• CAS No.: 943860-58-0
• Molecular Formula: C₃₃H₄₅N₃O₅Si
• Molecular Weight: 591.823

Synonyms:1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

Chemical Property of 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

There total 1 articles about 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol (881895-05-2) + tert-butyldimethylsilyl chloride (18162-48-6) → 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol (943860-58-0)

Guidance literature:

With dmap; In pyridine; at 20 ℃;

DOI:10.1055/s-2007-966022

Reference yield: 97.0%

1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol (943860-58-0) + methanesulfonyl chloride (124-63-0) → 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol (943860-54-6)

Guidance literature:

With pyridine; at 20 ℃; for 3h;

DOI:10.1055/s-2007-966022

Reference yield: 91.0%

1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol (943860-58-0) → 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-5-oxo-D-altritol (943860-59-1)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃;

DOI:10.1055/s-2007-966022

upstream raw materials:

2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

tert-butyldimethylsilyl chloride

Downstream raw materials:

1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-5-oxo-D-altritol

1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-5-O-methanesulfonyl-3,4,6-tri-O-benzyl-D-altritol

(2S,3S,4R,5S)-3,4-bis(benzyloxy)-2-[(benzyloxy)methyl]-5-[(tert-butyldimethylsiloxy)methyl]pyrrolidine

C₃₈H₅₃NO₆Si

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 943860-58-0 1-O-(tert-butyldimethylsilyl)-2-deoxy-2-azido-3,4,6-tri-O-benzyl-D-altritol

Send

Send

Metric Ton KG G Pound L ML

Send

Send