N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

Base Information

Chemical Name:N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide
CAS No.:1059145-62-8
Molecular Formula:C₂₃H₂₄N₄O₃S
Molecular Weight:436.535
Hs Code.:

Synonyms:N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

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Chemical Property of N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

Chemical Property:

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Technology Process of N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

There total 4 articles about N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1059147-41-9
benzyl 2-(4-((N-(pyridin-2-ylmethyl)phenylsulfonamido)-methyl)benzoyl)pyrazolidine-1-carboxylate

: 1059145-62-8
N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; for 16h;

Reference yield:

: 1059147-36-2
benzyl 2-(4-(aminomethyl)benzoyl)pyrazolidine-1-carboxylate

: 1059145-62-8
N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 1.5 h / 50 °C

1.2: 1 h / 0 °C

2.1: triethylamine / tetrahydrofuran / 4 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h

With hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol;

Reference yield:

: 1059147-35-1
benzyl 2-(4-((tert-butoxycarbonyl)methyl)benzoyl)-pyrazolidine-1-carboxylate

: 1059145-62-8
N-(4-(pyrazolidine-1-carbonyl)benzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

2.1: methanol / 1.5 h / 50 °C

2.2: 1 h / 0 °C

3.1: triethylamine / tetrahydrofuran / 4 h / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h

With hydrogen; triethylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;