(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene

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Chemical Name:(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene
CAS No.:1202242-76-9
Molecular Formula:C₃₄H₄₆N₂O₄
Molecular Weight:546.75
Hs Code.:

Synonyms:(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene

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Chemical Property of (6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene

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Technology Process of (6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene

There total 5 articles about (6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

: 1202242-80-5
(2S,9S)-4,7-di-[N-(S)-α-phenylethyl]-4,7-diaza-2,9-decanediol

: 1202242-76-9
(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-dimethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene

Guidance literature:: (2S,9S)-4,7-di-[N-(S)-α-phenylethyl]-4,7-diaza-2,9-decanediol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere; Reflux;

bis(o-phenylene)glycol ditosylate; In tetrahydrofuran; at 0 ℃; for 50.5h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.09.010