1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one]

Base Information

• Chemical Name: 1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one]
• CAS No.: 1620631-21-1
• Molecular Formula: C₃₁H₂₈O₁₀
• Molecular Weight: 560.557

Synonyms:1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one]

Chemical Property of 1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one]

Chemical Property:

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Technology Process of 1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one]

There total 2 articles about 1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + phloridizin (60-81-1,6426-09-1,40816-73-7,130549-93-8,138665-98-2) → 3-(4-Hydroxy-phenyl)-1-(2,4,6-trihydroxy-phenyl)-propan-1-on (60-82-2) + 1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one] (1620631-21-1) + methylenebisphloridzin + deglucosylmethylenebisphloridzin

Guidance literature:

With dielectric barrier discharge plasma;

Reference yield:

3-(4-Hydroxy-phenyl)-1-(2,4,6-trihydroxy-phenyl)-propan-1-on (60-82-2) + chloromethyl methyl ether (107-30-2) → 1,1'-[methylenebis(2,4,6-trihydroxy-3,1-phenylene)]bis[3-(4-hydroxyphenyl)propan-1-one] (1620631-21-1)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃;

DOI:10.1002/ejoc.201400104

upstream raw materials:

3-(4-Hydroxy-phenyl)-1-(2,4,6-trihydroxy-phenyl)-propan-1-on

chloromethyl methyl ether

methanol

phloridizin

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