N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

Base Information

Chemical Name:N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide
CAS No.:1361414-06-3
Molecular Formula:C₂₅H₂₃F₃N₂O₃S
Molecular Weight:488.53
Hs Code.:

Synonyms:N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

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Chemical Property of N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

Chemical Property:

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Technology Process of N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

There total 5 articles about N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ammonium thiocyanate

: 17061-62-0
N,N-bis(p-methoxybenzyl)amine

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 1361414-06-3
N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

Guidance literature:: ammonium thiocyanate; 3-(Trifluoromethyl)benzoyl chloride; In acetone; at 0 ℃; for 1h;

N,N-bis(p-methoxybenzyl)amine; In acetone; at 0 ℃; for 0.5h;

Reference yield:

: 17061-62-0
N,N-bis(p-methoxybenzyl)amine

: 1147550-11-5
ammonium thiocyanate

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 1361414-06-3
N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

Guidance literature:: ammonium thiocyanate; 3-(Trifluoromethyl)benzoyl chloride; In acetone; at 0 ℃; for 1.16667h;

N,N-bis(p-methoxybenzyl)amine; In acetone; at 0 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2018.03.001

Reference yield:

: 2557-13-3
3-trifluoromethylbenzoic acid methyl ester

: 1361414-06-3
N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-(trifluoromethyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol / 20 °C

1.2: pH 2

2.1: thionyl chloride / dichloromethane / 2 h / 40 °C

3.1: acetone / 2 h / 0 °C

3.2: 1 h / 0 °C

With thionyl chloride; sodium hydroxide; In methanol; dichloromethane; acetone;