(1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

Base Information

Chemical Name:(1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine
CAS No.:1134563-96-4
Molecular Formula:C₁₆H₂₅NO₃
Molecular Weight:279.379
Hs Code.:

Synonyms:(1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

Chemical Property:

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Technology Process of (1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

There total 2 articles about (1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64-19-7,77671-22-8
acetic acid

: 514168-47-9
(S)-1-((R)-2-Methoxy-1-phenyl-ethyl)-2-propyl-aziridine

: 1134563-96-4
(1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

Guidance literature:: In toluene; for 4h; regioselective reaction; Reflux;
DOI:10.3987/COM-08-11537

Reference yield: 72.0%

: 75-36-5
acetyl chloride

: 514168-48-0
(S)-2-Isopropyl-1-((R)-2-methoxy-1-phenyl-ethyl)-aziridine

: 1134563-96-4
(1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

: 1134564-10-5
(2S,1'R)-N-(2'-methoxy-1'-phenylethyl)-2-acetoxy-3-methylbutylamine

Guidance literature:: acetyl chloride; (S)-2-Isopropyl-1-((R)-2-methoxy-1-phenyl-ethyl)-aziridine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

With water; In tetrahydrofuran; at 20 ℃; for 0.333333h; regioselective reaction; Inert atmosphere;
DOI:10.3987/COM-08-11537

Reference yield:

: 1134563-96-4
(1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine

: 2026-48-4,473-75-6
(S)-valinol

Guidance literature:: (1S,1'R)-N-(2'-methoxy-1'-phenylethyl)-1-acetoxymethyl-2-methylpropylamine; With palladium dihydroxide; hydrogen;

With hydrogenchloride; In water;
DOI:10.3987/COM-08-11537