2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt

Base Information

Chemical Name:2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt
CAS No.:865436-03-9
Molecular Formula:C₂HF₃O₂*C₃₂H₃₉N₅O₇S
Molecular Weight:751.781
Hs Code.:

2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt

Synonyms:2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt

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Chemical Property of 2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt

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Technology Process of 2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt

There total 1 articles about 2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 865436-11-9
2S,4R,20S-3-[tert-butoxycarbonyl-(2-(5-[(tert-butoxycarbonyl-pyridin-2-yl-amino)-methyl]-pyrrolidin-3-yloxy)-acetyl)-amino]-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 103-80-0
phenylacetyl chloride

: 865436-03-9
2S,4R,20S-3-(2-[1-phenylacetyl-5-(pyridin-2-ylaminomethyl)-pyrrolidin-3-yloxy]-acetylamino)-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid TFA-salt

Guidance literature:: 2S,4R,20S-3-[tert-butoxycarbonyl-(2-(5-[(tert-butoxycarbonyl-pyridin-2-yl-amino)-methyl]-pyrrolidin-3-yloxy)-acetyl)-amino]-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid tert-butyl ester; phenylacetyl chloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

trifluoroacetic acid; at 20 ℃; for 4h;