Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

Base Information

Chemical Name:Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside
CAS No.:331281-74-4
Molecular Formula:C₃₆H₃₇ClO₇S
Molecular Weight:649.205
Hs Code.:

Synonyms:Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

Suppliers and Price of Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

There total 1 articles about Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7693-45-0
4-Chlorophenyl chloroformate

: 180187-58-0
ethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 331281-74-4
Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 72.0%

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 331281-74-4
Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

: 331281-75-5
3,4,6-Tri-O-benzyl-2-para-chlorophenylcarbonyl-β-D-glucopyranosyl-(1->6)-1,2:3,4-diisopropylidene-α-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; methyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 5h;

Reference yield:

: 331281-74-4
Thioethyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucopyranoside

: 40246-33-1
3,4,6-tri-O-benzyl-β-D-glucopyranoside-(1->6)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / MeOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 5 h / 0 °C

2: 87 percent / aq. LiOH; H₂O₂ / tetrahydrofuran / 1 h / 0 °C

With lithium hydroxide; 4 A molecular sieve; dihydrogen peroxide; methyl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;