C₂₀H₃₀O₄S

Base Information

Chemical Name:C₂₀H₃₀O₄S
CAS No.:1300656-02-3
Molecular Formula:C₂₀H₃₀O₄S
Molecular Weight:366.522
Hs Code.:

C<sub>20</sub>H<sub>30</sub>O<sub>4</sub>S

Synonyms:C₂₀H₃₀O₄S

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Chemical Property of C₂₀H₃₀O₄S

Chemical Property:

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Technology Process of C₂₀H₃₀O₄S

There total 3 articles about C₂₀H₃₀O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1072220-37-1
(3aS,7aS)-1,3-bis(4-bromobenzyl)-2-((E)-but-2-enyl)-2-chloro-octahydro-1H-benzo[d]-[1,3,2]-diazasilole

: 1300656-01-2
C₁₆H₂₂O₄S

: 1300656-02-3
C₂₀H₃₀O₄S

Guidance literature:: (3aS,7aS)-1,3-bis(4-bromobenzyl)-2-((E)-but-2-enyl)-2-chloro-octahydro-1H-benzo[d]-[1,3,2]-diazasilole; C₁₆H₂₂O₄S; With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 0.25h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja201467z

Reference yield:

: C₉H₁₆O₂

: 1300656-02-3
C₂₀H₃₀O₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylamine hydrochloride; triethylamine / dichloromethane / 36 h / Inert atmosphere

2.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 3 h / 0 °C / Inert atmosphere

2.2: 0.25 h / 0 - 20 °C / Inert atmosphere

With trimethylamine hydrochloride; triethylamine; scandium tris(trifluoromethanesulfonate); In dichloromethane;
DOI:10.1021/ja201467z

Reference yield:

: 95273-27-1
(3S,4S)-4-hydroxy-3-methyl-1-hexene

: 1300656-02-3
C₂₀H₃₀O₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: Hoveyda-Grubbs catalyst second generation / chloroform / 24 h / Inert atmosphere; Reflux

2.1: trimethylamine hydrochloride; triethylamine / dichloromethane / 36 h / Inert atmosphere

3.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 3 h / 0 °C / Inert atmosphere

3.2: 0.25 h / 0 - 20 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; trimethylamine hydrochloride; triethylamine; scandium tris(trifluoromethanesulfonate); In dichloromethane; chloroform;
DOI:10.1021/ja201467z