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C47H64O13Si2

Base Information Edit
  • Chemical Name:C47H64O13Si2
  • CAS No.:1313275-26-1
  • Molecular Formula:C47H64O13Si2
  • Molecular Weight:893.188
  • Hs Code.:
  • Mol file:1313275-26-1.mol
C<sub>47</sub>H<sub>64</sub>O<sub>13</sub>Si<sub>2</sub>

Synonyms:C47H64O13Si2

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Chemical Property of C47H64O13Si2 Edit
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Technology Process of C47H64O13Si2

There total 58 articles about C47H64O13Si2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
dirhodium tetraacetate; In dichloromethane; at 23 ℃; for 0.166667h; Molecular sieve;
Guidance literature:
With dirhodium tetraacetate; In dichloromethane; at 23 ℃; for 2h; Molecular sieve;
DOI:10.1073/pnas.1015257108
Guidance literature:
Multi-step reaction with 11 steps
1.1: trimethylaluminum / toluene / 0.17 h / 0 °C
1.2: 7.75 h / 23 °C / Reflux
2.1: 13 h / 220 °C / Neat (no solvent)
3.1: potassium tert-butylate / dimethyl sulfoxide / 1.17 h / 23 - 120 °C
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 23 °C
5.1: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / tetrahydrofuran / 1 h / -78 °C
5.2: 17.5 h / -78 - 23 °C
5.3: 0.33 h / 23 °C
6.1: dichloromethane / 1.25 h / 0 - 23 °C
6.2: 40 h / 23 °C
7.1: lithium tert-butoxide / tetrahydrofuran / 0.08 h / -78 °C
7.2: 2.5 h / -78 - -22 °C
7.3: 4.5 h / -22 - 23 °C
8.1: 2,6-dimethylpyridine; sodium periodate; potassium osmate(VI) dihydrate / water; tetrahydrofuran / 2 h / 0 - 23 °C
9.1: bromocatecholborane / dichloromethane / 0.75 h / -78 °C
9.2: -78 - 23 °C
10.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 1.33 h / 23 - 55 °C
11.1: tetrakis(actonitrile)copper(I) hexafluorophosphate / dichloromethane / 2.67 h / 23 °C / Molecular sieve
With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; N,N,N,N,-tetramethylethylenediamine; bromocatecholborane; potassium tert-butylate; trimethylaluminum; tert.-butyl lithium; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; lithium tert-butoxide; tetrakis(actonitrile)copper(I) hexafluorophosphate; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
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