3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

Base Information

Chemical Name:3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester
CAS No.:943345-10-6
Molecular Formula:C₂₈H₂₂N₂O₆
Molecular Weight:482.492
Hs Code.:

Synonyms:3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

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Chemical Property of 3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

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Technology Process of 3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

There total 5 articles about 3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943344-64-7
3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenol

: 96-32-2
bromoacetic acid methyl ester

: 943345-10-6
3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

Guidance literature:: With caesium carbonate; for 0.75h; Reflux;

Reference yield:

: 4254-17-5
4-methoxybenzoin

: 943345-10-6
3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Cooling with ice

2.1: acetic anhydride / 0 °C

2.2: 10 - 130 °C

3.1: trichlorophosphate / 1 h / Reflux

3.2: 55 - 75 °C / pH 9

4.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 120 °C

5.1: caesium carbonate / 0.75 h / Reflux

With acetic anhydride; caesium carbonate; diethylamine; trichlorophosphate; In N,N-dimethyl-formamide;

Reference yield:

: 14774-62-0
2-amino-4-(4-methoxyphenyl)-5-phenylfuran-3-carbonitrile

: 943345-10-6
3-{[5-(4-methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]oxy}phenoxyacetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride / 0 °C

1.2: 10 - 130 °C

2.1: trichlorophosphate / 1 h / Reflux

2.2: 55 - 75 °C / pH 9

3.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 120 °C

4.1: caesium carbonate / 0.75 h / Reflux

With acetic anhydride; caesium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;