tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)

Base Information

Chemical Name:tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)
CAS No.:1213265-97-4
Molecular Formula:C₃₆H₄₀Cl₄N₂Ti
Molecular Weight:690.419
Hs Code.:

Synonyms:tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)

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Chemical Property of tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)

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Technology Process of tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)

There total 1 articles about tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7550-45-0
titanium tetrachloride

: 153625-67-3
1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene

: 1213265-97-4
tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)

Guidance literature:: In dichloromethane; under Ar or N2; ligand added to CH2Cl2; frozen in liq. N2; neat TiCl4 added upon thawing; warmed slowly to 25°C with stirring; stirred for 1 h; solvent removed under reduced pressure; washed with pentane; elem. anal.;
DOI:10.1021/ic902101z

Reference yield: 85.0%

: 1213265-97-4
tetrachloro(N,N'-bis(2,6-diisopropylphenylimino)acenaphthylene)titanium(IV)

: 7412-67-1
neopentyl lithium

: [(N,N'-bis(2,6-diisopropylphenylamido)acenaphthylene)Ti(neopentyl)₂]

Guidance literature:: In pentane; at 20 ℃; for 1h; Mechanism; Inert atmosphere; Schlenk technique; Glovebox; Cooling with liquid nitrogen;
DOI:10.1021/acs.inorgchem.6b00404