C₁₄H₁₅NO₄S

Base Information

• Chemical Name: C₁₄H₁₅NO₄S
• CAS No.: 1310415-39-4
• Molecular Formula: C₁₄H₁₅NO₄S
• Molecular Weight: 293.343
• Mol file: 1310415-39-4.mol

Synonyms:C₁₄H₁₅NO₄S

Chemical Property of C₁₄H₁₅NO₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₅NO₄S

There total 5 articles about C₁₄H₁₅NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H19NO3 (898404-90-5) → C14H15NO4S (1310415-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

2: tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; mineral oil;

DOI:10.1021/ol201236j

Reference yield:

ethyl 1-aminocyclopent-3-ene-1-carboxylate (199532-88-2) → C14H15NO4S (1310415-39-4)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / water / Inert atmosphere

2: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

4: tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

With lithium borohydride; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; water; mineral oil;

DOI:10.1021/ol201236j

Reference yield:

ethyl 1-((4-bromobenzylidene)amino)cyclopent-3-ene-1-carboxylate (199532-83-7) → C14H15NO4S (1310415-39-4)

Guidance literature:

Multi-step reaction with 5 steps

1.1: hydrogenchloride; water / Inert atmosphere

1.2: Inert atmosphere

2.1: sodium hydrogencarbonate / water / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

5.1: tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium borohydride; water; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; water; mineral oil; 1.2: Fischer esterification;

DOI:10.1021/ol201236j

upstream raw materials:

C₁₁H₁₉NO₃

p-toluenesulfonyl chloride

ethyl 1-aminocyclopent-3-ene-1-carboxylate

ethyl 1-((tert-butoxycarbonyl)amino)cyclopent-3-ene-1-carboxylate

Downstream raw materials:

C₁₄H₁₅NO₅S

C₁₇H₂₃NO₅SSi

1-tosyl-3-oxa-1-azaspiro[4.4]non-8-ene-2,7-dione

C₂₀H₂₇NO₅SSi