C₂₄H₂₇N₅O₅S

Base Information

Chemical Name:C₂₄H₂₇N₅O₅S
CAS No.:1346245-15-5
Molecular Formula:C₂₄H₂₇N₅O₅S
Molecular Weight:497.575
Hs Code.:

C<sub>24</sub>H<sub>27</sub>N<sub>5</sub>O<sub>5</sub>S

Synonyms:C₂₄H₂₇N₅O₅S

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Chemical Property of C₂₄H₂₇N₅O₅S

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Technology Process of C₂₄H₂₇N₅O₅S

There total 14 articles about C₂₄H₂₇N₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1346242-80-5
C₂₃H₂₅N₅O₃

: 124-63-0
methanesulfonyl chloride

: 1346245-15-5
C₂₄H₂₇N₅O₅S

Guidance literature:: With triethylamine; In dichloromethane; at 5 ℃; for 1h; Inert atmosphere;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346245-15-5
C₂₄H₂₇N₅O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate / 2 h / 100 °C

1.2: Cooling with ice

2.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux

3.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

4.2: 5 - 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

5.2: Cooling with ice

6.1: triethylamine / dichloromethane / 1 h / 5 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; sodium carbonate; triethylamine; sodium t-butanolate; trichlorophosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1083325-87-4
7‐bromo‐2‐(1‐methyl‐1H‐pyrazol‐4‐yl)quinoxaline

: 1346245-15-5
C₂₄H₂₇N₅O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

2.2: 5 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3.2: Cooling with ice

4.1: triethylamine / dichloromethane / 1 h / 5 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; triethylamine; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; mineral oil;