C₃₄H₄₆N₂O₄S

Base Information

Chemical Name:C₃₄H₄₆N₂O₄S
CAS No.:1428427-75-1
Molecular Formula:C₃₄H₄₆N₂O₄S
Molecular Weight:578.816
Hs Code.:

C<sub>34</sub>H<sub>46</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₃₄H₄₆N₂O₄S

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Chemical Property of C₃₄H₄₆N₂O₄S

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Technology Process of C₃₄H₄₆N₂O₄S

There total 16 articles about C₃₄H₄₆N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1428427-71-7
C₃₄H₄₂N₂O₄S

: 1428427-75-1
C₃₄H₄₆N₂O₄S

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In isopropyl alcohol; for 24h; Inert atmosphere;
DOI:10.1021/ol400469w

Reference yield:

: C₃₆H₄₃NO₃Si

: 1428427-75-1
C₃₄H₄₆N₂O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

4: copper(II) sulfate / toluene / 12 h / 20 °C / Inert atmosphere

5: tetrahydrofuran; chlorobenzene / 1 h / Inert atmosphere; Reflux

6: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 24 h / Inert atmosphere

With palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; Dess-Martin periodane; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; chlorobenzene; isopropyl alcohol; toluene; 5: |Grignard Reaction;
DOI:10.1021/ol400469w

Reference yield:

: 145032-58-2
ethyl (1S,5R)-2-oxo-3-oxabicyclo[3.1.0]hexane-1-carboxylate

: 1428427-75-1
C₃₄H₄₆N₂O₄S

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / -40 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / dichloromethane / 48 h / 0 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

4.2: 0.5 h / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / ethanol / 12 h / 55 °C / Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

7.1: tetrahydrofuran / 13 h / Inert atmosphere; Reflux

8.1: lithium borohydride / ethanol / 4 h / Inert atmosphere

9.1: palladium 10% on activated carbon; ammonium formate / methanol / 12.5 h / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / Inert atmosphere

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / Inert atmosphere

12.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

13.1: copper(II) sulfate / toluene / 12 h / 20 °C / Inert atmosphere

14.1: tetrahydrofuran; chlorobenzene / 1 h / Inert atmosphere; Reflux

15.1: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 24 h / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; lithium borohydride; n-butyllithium; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; ammonium formate; pyridinium p-toluenesulfonate; Dess-Martin periodane; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; isopropyl alcohol; toluene; 14.1: |Grignard Reaction;
DOI:10.1021/ol400469w