Technology Process of C10H7ClO2
There total 3 articles about C10H7ClO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphorus trichloride;
In
diethyl ether; N,N-dimethyl-formamide;
at 5 - 10 ℃;
DOI:10.1016/j.bmc.2011.01.051
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / tetrahydrofuran / 20 °C / Cooling with ice
2: phosphorus trichloride / diethyl ether; N,N-dimethyl-formamide / 5 - 10 °C
With
sodium hydride; phosphorus trichloride;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
1: Dieckmann reaction;
DOI:10.1016/j.bmc.2011.01.051
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium ethanolate / ethanol / 0.17 h / 25 °C
1.2: Reflux
2.1: sodium hydride / tetrahydrofuran / 20 °C / Cooling with ice
3.1: phosphorus trichloride / diethyl ether; N,N-dimethyl-formamide / 5 - 10 °C
With
sodium ethanolate; sodium hydride; phosphorus trichloride;
In
tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide;
2.1: Dieckmann reaction;
DOI:10.1016/j.bmc.2011.01.051