methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate

Base Information

Chemical Name:methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate
CAS No.:80256-17-3
Molecular Formula:C₁₉H₂₈O₄Si
Molecular Weight:348.514
Hs Code.:

Synonyms:methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate

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Chemical Property of methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate

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Technology Process of methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate

There total 2 articles about methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107-21-1
ethylene glycol

: 80256-16-2
methyl 3-dimethylphenylsilyl-4-methyl-5-oxocyclohexanecarboxylate

: 80256-17-3
methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate

Guidance literature:: With toluene-4-sulfonic acid; In various solvent(s); for 2.5h; Heating;
DOI:10.1039/P19810002520

Reference yield:

: 3839-31-4
dimethyl(phenyl)silyllithium

: 80256-17-3
methyl 5,5-ethylenedioxy-4-methyl-3-dimethylphenylsilylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) copper(I) iodide, 2.) HMPA / 1.) THF, -23 deg C, 5 h, 2.) room temperature, 3 h

2: 95 percent / toluene-p-sulphonic acid / various solvent(s) / 2.5 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; toluene-4-sulfonic acid; In various solvent(s);
DOI:10.1039/P19810002520