2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose
CAS No.:75719-88-9
Molecular Formula:C₅₅H₅₇N₃O₁₁
Molecular Weight:936.071
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

Suppliers and Price of 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

There total 2 articles about 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37700-64-4
(5S)-5-benzyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triazadodecan-12-oic acid

: 75719-88-9
2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / dicyclohexylcarbodi-imide / dimethylformamide

2: imidazole / dimethylformamide / 24 h / Ambient temperature

With 1H-imidazole; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85517-2

Reference yield:

: 6564-72-3
2,3,4,6-tetra-O-benzyl-D-glucopyranose

: 75719-85-6
N-benzyloxycarbonyl-L-phenylalanylglycylglycine pentachlorophenyl ester

: 75719-88-9
2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

: 75719-89-0
2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-α-D-glucopyranose

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 24h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0008-6215(00)85517-2

Reference yield: 92.0%

: 6153-56-6
oxalic acid dihydrate

: 75719-88-9
2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonyl-L-phenylalanylglycylglycyl)-β-D-glucopyranose

: 75720-06-8
1-O-(L-phenylalanylglycylglycyl)-β-D-glucopyranose mono-oxalate

Guidance literature:: With hydrogen; palladium on activated charcoal; In 2-methoxy-ethanol; acetic acid; for 20h;
DOI:10.1016/S0008-6215(00)85517-2