{[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

Base Information

Chemical Name:{[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid
CAS No.:103497-72-9
Molecular Formula:C₃₀H₂₉N₃O₁₂
Molecular Weight:623.573
Hs Code.:

Synonyms:{[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

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Chemical Property of {[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

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Technology Process of {[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

There total 4 articles about {[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103471-61-0
({2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-[methoxy-(2-nitro-phenyl)-methyl]-phenyl}-carboxymethyl-amino)-acetic acid

: 103497-72-9
{[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

Guidance literature:: With hydrogenchloride; 3-(N-morpholino)propanesulfonic acid; K₂H₂EGTA; potassium chloride; 2-amino-2-hydroxymethyl-1,3-propanediol; In water; at 22 ℃; Irradiation;
DOI:10.1021/ja00218a034

Reference yield:

: 20627-73-0
1-(dimethoxymethyl)-2-nitrobenzene

: 103497-72-9
{[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) trimethylsilyl trifluoromethanesulfonate, 2,6-di-tert-butylpyridine; 2.) tetrabutylammonium fluoride trihydrate / 1.) CHCl₃, room temp.; 2.) CHCl₃, room temp., 15 min.

2: 1M KOH then acid / dioxane; methanol; H₂O

3: KCl, Tris, MOPS, K₂H₂EGTA, HCl / H₂O / 22 °C / Irradiation

With hydrogenchloride; 3-(N-morpholino)propanesulfonic acid; potassium hydroxide; 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; K₂H₂EGTA; potassium chloride; tetrabutyl ammonium fluoride; 2-amino-2-hydroxymethyl-1,3-propanediol; In 1,4-dioxane; methanol; water;
DOI:10.1021/ja00218a034

Reference yield:

: 96315-10-5
N-(2-(2-(2-(bis(methoxycarbonylmethyl)amino)phenoxy)ethoxy)-4-methylphenyl)-N-(methoxycarbonylmethyl)aminoacetic acid methyl ester

: 103497-72-9
{[2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-(2-nitroso-benzoyl)-phenyl]-carboxymethyl-amino}-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) trimethylsilyl trifluoromethanesulfonate, 2,6-di-tert-butylpyridine; 2.) tetrabutylammonium fluoride trihydrate / 1.) CHCl₃, room temp.; 2.) CHCl₃, room temp., 15 min.

2: 1M KOH then acid / dioxane; methanol; H₂O

3: KCl, Tris, MOPS, K₂H₂EGTA, HCl / H₂O / 22 °C / Irradiation

With hydrogenchloride; 3-(N-morpholino)propanesulfonic acid; potassium hydroxide; 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; K₂H₂EGTA; potassium chloride; tetrabutyl ammonium fluoride; 2-amino-2-hydroxymethyl-1,3-propanediol; In 1,4-dioxane; methanol; water;
DOI:10.1021/ja00218a034