3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

Base Information

Chemical Name:3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide
CAS No.:1434817-41-0
Molecular Formula:C₁₆H₁₅F₃N₂OS
Molecular Weight:340.369
Hs Code.:

Synonyms:3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

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Chemical Property of 3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

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Technology Process of 3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

There total 5 articles about 3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 22282-99-1
4-bromo-2-methylpyridine

: 1434817-47-6
3-(4-bromo-2-trifluoromethyl-phenylsulfanyl)propionamide

: 1434817-41-0
3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

Guidance literature:: 4-bromo-2-methylpyridine; With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; bis(pinacol)diborane; In N,N-dimethyl-formamide; at 80 ℃; for 22h;

3-(4-bromo-2-trifluoromethyl-phenylsulfanyl)propionamide; With potassium carbonate; In water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In N,N-dimethyl-formamide; at 60 ℃; for 20h;

Reference yield: 71.0%

: 22282-99-1
4-bromo-2-methylpyridine

: 1434817-47-6
3-(4-bromo-2-trifluoromethyl-phenylsulfanyl)propionamide

: 73183-34-3
bis(pinacol)diborane

: 1434817-41-0
3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

Guidance literature:: 4-bromo-2-methylpyridine; bis(pinacol)diborane; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 22h;

3-(4-bromo-2-trifluoromethyl-phenylsulfanyl)propionamide; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In water; N,N-dimethyl-formamide; at 20 - 60 ℃; for 20.5h;

Reference yield: 69.0%

: 660867-80-1
2-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

: 1434817-47-6
3-(4-bromo-2-trifluoromethyl-phenylsulfanyl)propionamide

: 1434817-41-0
3-[4-(2-methylpyridin-4-yl)-2-trifluoromethylphenylsulfanyl]propionamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In water; N,N-dimethyl-formamide; at 50 ℃; for 20h;