N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Base Information

Chemical Name:N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline
CAS No.:1393736-05-4
Molecular Formula:C₂₃H₂₁N₃O₅
Molecular Weight:419.437
Hs Code.:

Synonyms:N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Suppliers and Price of N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Chemical Property:

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Technology Process of N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

There total 3 articles about N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372129-84-4
5-chloro-N¹-(4-cyanophenyl)-4-methoxycarbonyl-2-nitroaniline

: 1393736-05-4
N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 190 °C / Microwave irradiation

2: lithium borohydride / tetrahydrofuran / 0.25 h / 20 °C

With lithium borohydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm3007678

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 1393736-05-4
N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; nitric acid / 2 h / 0 - 20 °C

2: sulfuric acid / 2 h / Reflux

3: potassium tert-butylate / N,N-dimethyl-formamide / 0 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 190 °C / Microwave irradiation

5: lithium borohydride / tetrahydrofuran / 0.25 h / 20 °C

With lithium borohydride; sulfuric acid; potassium tert-butylate; nitric acid; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm3007678

Reference yield:

: 19861-62-2
2,4-dichloro-5-nitrobenzoic acid

: 1393736-05-4
N-(4'-cyanophenyl)-5-(4-hydroxymethyl-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 2 h / Reflux

2: potassium tert-butylate / N,N-dimethyl-formamide / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 190 °C / Microwave irradiation

4: lithium borohydride / tetrahydrofuran / 0.25 h / 20 °C

With lithium borohydride; sulfuric acid; potassium tert-butylate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm3007678