7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

Base Information

Chemical Name:7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde
CAS No.:868660-45-1
Molecular Formula:C₁₈H₁₁FN₂O₃
Molecular Weight:322.295
Hs Code.:

Synonyms:7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

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Chemical Property of 7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

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Technology Process of 7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

There total 2 articles about 7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 868660-36-0
7-(4-fluorobenzyl)pyrano[3,4-b]pyrrolo[3,2-d]pyridin-4(7H)-one

: 33797-51-2
eschenmoser's salt

: 868660-45-1
7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

Guidance literature:: In DMF (N,N-dimethyl-formamide); at 130 ℃; for 4h; Microwave irradiation;

Reference yield: 64.0%

: 868660-36-0
7-(4-fluorobenzyl)pyrano[3,4-b]pyrrolo[3,2-d]pyridin-4(7H)-one

: 30354-18-8
N,N-dimethyl(methylene)ammonium chloride

: 868660-45-1
7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

Guidance literature:: In N,N-dimethyl-formamide; at 130 ℃; for 4h; Microwave irradiation;

Reference yield:

: 868660-45-1
7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde

: 10316-79-7
(1-aminocyclopentyl)methanol

: 3-(4-fluorobenzyl)-7-hydroxy-1-({[1-(hydroxymethyl)cyclopentyl]amino}methyl)-3,7-dihydro-6H-pyrrolo[2,3-c]-1,7-naphthyridin-6-one

Guidance literature:: 7-(4-fluorobenzyl)-4-oxo-4,7-dihydropyrano[3,4-b]pyrrolo[3,2-d]pyridine-9-carbaldehyde; (1-aminocyclopentyl)methanol; In dichloromethane; at 20 ℃; for 2h;

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 18 - 24h;

With hydroxylamine; In ethanol; for 3h; Heating / reflux;