8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide

Base Information

• Chemical Name: 8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide
• CAS No.: 856698-65-2
• Molecular Formula: C₂₁H₂₅N₃O₃
• Molecular Weight: 367.448

Synonyms:8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide

Chemical Property of 8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide

Chemical Property:

Purity/Quality:

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Technology Process of 8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide

There total 1 articles about 8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

8-hydroxy-2,3-dimethyl-7-(3-oxo-3-phenylpropyl)imidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide (498529-53-6) → 8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide (856698-65-2)

Guidance literature:

8-hydroxy-2,3-dimethyl-7-(3-oxo-3-phenylpropyl)imidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide; With potassium tert-butylate; RuCI₂[(R)-BINAP][(R)-DAIPEN]; In isopropyl alcohol; at 20 ℃; for 0.333333h; Autoclave;

With hydrogen; In isopropyl alcohol; at 20 ℃; for 22h; under 30003 Torr;

Reference yield: 42.0%

8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide (856698-65-2)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; for 0.05h;

Reference yield:

(3R)-8-hydroxy-7-(3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide (856449-27-9) + 8-hydroxy-7-((S)-3-hydroxy-3-phenylpropyl)-2,3-dimethylimidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide (856698-65-2) + (3S)-8-(tert-butyl-dimethylsilanyloxy)-7-(3-hydroxy-3-phenyl-propyl)-2,3-dimethyl-imidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide + (3R)-8-(tert-butyl-dimethylsilanyloxy)-7-(3-hydroxy-3-phenyl-propyl)-2,3-dimethyl-imidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide (856698-68-5) + (S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride (39637-99-5,20445-33-4) → C41H39F6N3O7 (1000293-68-4) + C41H39F6N3O7

Guidance literature:

With pyridine; In tetrachloromethane; dichloromethane; at 20 ℃; for 6h;

upstream raw materials:

8-hydroxy-2,3-dimethyl-7-(3-oxo-3-phenylpropyl)imidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide

Downstream raw materials:

(3R)-8-(tert-butyl-dimethylsilanyloxy)-7-(3-hydroxy-3-phenyl-propyl)-2,3-dimethyl-imidazo[1,2-a]pyridine-6-carboxylic acid dimethylamide

C₄₁H₃₉F₆N₃O₇

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