ethyl 4-methylbenzoyl carbonate

Base Information

• Chemical Name: ethyl 4-methylbenzoyl carbonate
• CAS No.: 14189-19-6
• Molecular Formula: C₁₁H₁₂O₄
• Molecular Weight: 208.214

Synonyms:ethyl 4-methylbenzoyl carbonate

Chemical Property of ethyl 4-methylbenzoyl carbonate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl 4-methylbenzoyl carbonate

There total 1 articles about ethyl 4-methylbenzoyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroformic acid ethyl ester (541-41-3) + p-Toluic acid (99-94-5) → ethyl 4-methylbenzoyl carbonate (14189-19-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; at -7 ℃; for 0.5h;

DOI:10.1055/s-1987-28035

Reference yield: 88.0%

ethyl 4-methylbenzoyl carbonate (14189-19-6) → 4-Methylbenzyl alcohol (589-18-4)

Guidance literature:

With methanol; sodium tetrahydroborate; In tetrahydrofuran; at 10 ℃; for 1h;

DOI:10.1055/s-1987-28035

Reference yield: 84.0%

2-Cyano-3N-(6-amino-2-pyridyl)aminopropenenitrile (37550-70-2) + ethyl 4-methylbenzoyl carbonate (14189-19-6) → 2-p-Tolyl-1,3,6,9b-tetraaza-phenalene-4-carbonitrile (121902-26-9)

Guidance literature:

at 130 ℃; for 3h;

upstream raw materials:

chloroformic acid ethyl ester

p-Toluic acid

Downstream raw materials:

2-p-Tolyl-1,9b-diaza-phenalene-7,9-dicarbonitrile

2-p-Tolyl-1,3,6,9b-tetraaza-phenalene

2-p-Tolyl-1,3,6,9b-tetraaza-phenalene-4-carboxylic acid ethyl ester

2-p-Tolyl-1,3,6,9b-tetraaza-phenalene-4-carbonitrile

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