trimethylgermyltriphenylsilane

Base Information

Chemical Name:trimethylgermyltriphenylsilane
CAS No.:27601-58-7
Molecular Formula:C₂₁H₂₄GeSi
Molecular Weight:377.097
Hs Code.:

Synonyms:trimethylgermyltriphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethylgermyltriphenylsilane

Chemical Property:

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Technology Process of trimethylgermyltriphenylsilane

There total 3 articles about trimethylgermyltriphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 76-86-8
Triphenylsilyl chloride

: 1529-47-1
chlorotrimethylgermane

: 993-52-2
hexamethyldigermane

: 27601-58-7
trimethylgermyltriphenylsilane

Guidance literature:: In tetrahydrofuran; Electrochem. Process; electroreduction, 3 F/mol electricity based on Me3GeCl, presence of LiClO4, molar ratio 1:2, Mg cathode and anode, sonication;
DOI:10.1039/c39920000896

Reference yield:

: 76-86-8
Triphenylsilyl chloride

: 1529-47-1
chlorotrimethylgermane

: 27601-58-7
trimethylgermyltriphenylsilane

Guidance literature:: With Na; In tetrahydrofuran; addn. of Ph3SiCl and naphthalene to a slurry of Na in THF, stirring for 20 h, addn. of the mixture at 0°C to Me3GeCl in THF, stirring for 1 h and warming to room temp.; evapn. (vac.) and extn. and recrystn. from hexane-CH2Cl2;
DOI:10.1016/0022-328X(90)87051-E