all-trans-N-Retinoylglycine ethyl ester

Base Information

Chemical Name:all-trans-N-Retinoylglycine ethyl ester
CAS No.:81425-66-3
Molecular Formula:C₂₄H₃₅NO₃
Molecular Weight:385.547
Hs Code.:

Synonyms:all-trans-N-Retinoylglycine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of all-trans-N-Retinoylglycine ethyl ester

Chemical Property:

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Technology Process of all-trans-N-Retinoylglycine ethyl ester

There total 2 articles about all-trans-N-Retinoylglycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 302-79-4
all-trans-retinoic-acid

: 459-73-4
GlyOEt*HCl

: 81425-66-3
all-trans-N-Retinoylglycine ethyl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1021/jm200256g

Reference yield:

: 302-79-4
all-trans-retinoic-acid

: 81425-66-3
all-trans-N-Retinoylglycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride / benzene / 4 h / 25 - 30 °C

2: 1.) aq. NaOH, potassium carbonate / 1.) ether, 4 deg C, 2.) benzene, 10 deg C, 1 h

With sodium hydroxide; potassium carbonate; phosphorus trichloride; In benzene;
DOI:10.1002/jps.2600730610