pentyl cyclohex-1-enecarboxylate

Base Information

Chemical Name:pentyl cyclohex-1-enecarboxylate
CAS No.:1293370-58-7
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:

Synonyms:pentyl cyclohex-1-enecarboxylate

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Chemical Property of pentyl cyclohex-1-enecarboxylate

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Technology Process of pentyl cyclohex-1-enecarboxylate

There total 2 articles about pentyl cyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 71-41-0
pentan-1-ol

: 201230-82-2
carbon monoxide

: 22524-46-5
cyclohex-1-en-1-yl 4-methylbenzenesulfonate

: 1293370-58-7
pentyl cyclohex-1-enecarboxylate

Guidance literature:: With potassium phosphate; palladium diacetate; In toluene; at 100 ℃; for 14h; under 5171.62 Torr; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol200744s

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1293370-58-7
pentyl cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium t-butanolate / tetrahydrofuran / -20 - 20 °C / Inert atmosphere

1.2: 1.5 h / -15 - -5 °C / Inert atmosphere

2.1: potassium phosphate; palladium diacetate / toluene / 14 h / 100 °C / 5171.62 Torr / Inert atmosphere; Molecular sieve

With potassium phosphate; palladium diacetate; sodium t-butanolate; In tetrahydrofuran; toluene;
DOI:10.1021/ol200744s