tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

Base Information

Chemical Name:tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane
CAS No.:908124-95-8
Molecular Formula:C₂₁H₃₂OSi
Molecular Weight:328.57
Hs Code.:

<i>tert</i>-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

Synonyms:tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

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Chemical Property of tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

Chemical Property:

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Technology Process of tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

There total 4 articles about tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 908125-52-0
2,4-dimethyl-2-phenylethynyl-pent-4-enoic acid ethyl ester

: 908124-95-8
tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0 °C

2: imidazole / CH₂Cl₂

With 1H-imidazole; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;
DOI:10.1021/ja063384n

Reference yield:

: 1483-82-5
phenylethynyl chloride

: 908124-95-8
tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA; HMPA / tetrahydrofuran; petroleum ether / -78 - 0 °C

1.2: 72 percent / tetrahydrofuran; petroleum ether / -78 - 20 °C

2.1: LiAlH₄ / diethyl ether / 0 °C

3.1: imidazole / CH₂Cl₂

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; Petroleum ether;
DOI:10.1021/ja063384n

Reference yield:

: 90646-75-6
ethyl 2,4-dimethyl-4-pentenoate

: 908124-95-8
tert-butyl-(2,4-dimethyl-2-phenylethynyl-pent-4-enyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA; HMPA / tetrahydrofuran; petroleum ether / -78 - 0 °C

1.2: 72 percent / tetrahydrofuran; petroleum ether / -78 - 20 °C

2.1: LiAlH₄ / diethyl ether / 0 °C

3.1: imidazole / CH₂Cl₂

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; Petroleum ether;
DOI:10.1021/ja063384n