tris(2,6-dimethoxyphenyl)phosphine selenide

Base Information

• Chemical Name: tris(2,6-dimethoxyphenyl)phosphine selenide
• CAS No.: 103661-68-3
• Molecular Formula: C₂₄H₂₇O₆PSe
• Molecular Weight: 521.409
• Mol file: 103661-68-3.mol

Synonyms:tris(2,6-dimethoxyphenyl)phosphine selenide

Chemical Property of tris(2,6-dimethoxyphenyl)phosphine selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tris(2,6-dimethoxyphenyl)phosphine selenide

There total 1 articles about tris(2,6-dimethoxyphenyl)phosphine selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tris(2,6-dimethoxyphenyl)phosphine (85417-41-0) → tris(2,6-dimethoxyphenyl)phosphine selenide (103661-68-3)

Guidance literature:

With selenium; In chloroform; for 5h; Heating;

DOI:10.1039/DT9850002505

Reference yield: 91.0%

1-iodo-butane (542-69-8) + tris(2,6-dimethoxyphenyl)phosphine selenide (103661-68-3) → C28H36O6PSe(1+)*I(1-)

Guidance literature:

In methanol; at -30 ℃; for 4h;

DOI:10.1246/bcsj.69.655

Reference yield:

1-bromo-butane (109-65-9) + tris(2,6-dimethoxyphenyl)phosphine selenide (103661-68-3) → Butyl-tris-(2,6-dimethoxy-phenyl)-phosphonium; perchlorate + C28H36O6PSe(1+)*ClO4(1-)

Guidance literature:

With perchloric acid; In methanol; at -30 ℃; for 18h; Yields of byproduct given;

DOI:10.1246/bcsj.69.655

upstream raw materials:

tris(2,6-dimethoxyphenyl)phosphine