3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI)

Base Information

Chemical Name:3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI)
CAS No.:84854-00-2
Molecular Formula:C₇H₆ClNO₂
Molecular Weight:171.583
Hs Code.:2933399090
Mol file:84854-00-2.mol

Synonyms:3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI)

Suppliers and Price of 3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI)

Chemical Property:

Boiling Point:325.2±31.0 °C(Predicted)
PKA:-3.26±0.62(Predicted)
PSA：39.07000
Density:1.375±0.06 g/cm3(Predicted)
LogP:0.76430

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI)

There total 2 articles about 3-Pyridinecarbonyl chloride, 1,2-dihydro-1-methyl-2-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15506-18-0
1-methyl-2-oxo-1,2-dihydropyridine-3-carboxylic acid

: 84854-00-2
1-Methyl-2-oxo-1,2-dihydro-pyridine-3-carbonyl chloride

Guidance literature:: With thionyl chloride; for 1.5h; Heating;

Reference yield:

: 609-71-2
2-hydroxy-3-carboxypyridine

: 84854-00-2
1-Methyl-2-oxo-1,2-dihydro-pyridine-3-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / H₂O; methanol / Heating

2: SOCl₂ / toluene / 80 °C

With potassium hydroxide; thionyl chloride; In methanol; water; toluene;
DOI:10.1246/bcsj.78.1127