methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

Base Information

Chemical Name:methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate
CAS No.:1178976-86-7
Molecular Formula:C₁₄H₂₅NO₇S
Molecular Weight:351.421
Hs Code.:

Synonyms:methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

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Chemical Property of methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

Chemical Property:

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Technology Process of methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

There total 3 articles about methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917887-43-5
syn-1-[N-(t-butoxycarbonyl)amino]-4-hydroxycyclohexane-1-carboxylic acid methyl ester

: 124-63-0
methanesulfonyl chloride

: 1178976-86-7
methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 10 - 20 ℃;

Reference yield:

: 285996-76-1
1-((tert-butoxycarbonyl)amino)-4-oxocyclohexanecarboxylic acid

: 1178976-86-7
methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

2: water; sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 10 - 20 °C

With sodium tetrahydroborate; water; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 191111-27-0
methyl 1-((tert-butoxycarbonyl)amino)-4-oxocyclohexanecarboxylate

: 1178976-86-7
methyl cis-1-tert.-butoxycarbonylamino-4-methanesulphonyloxy-cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 10 - 20 °C

With sodium tetrahydroborate; water; triethylamine; In tetrahydrofuran; dichloromethane;