C₂₁H₃₄O₂Si

Base Information

Chemical Name:C₂₁H₃₄O₂Si
CAS No.:1415231-57-0
Molecular Formula:C₂₁H₃₄O₂Si
Molecular Weight:346.585
Hs Code.:

C<sub>21</sub>H<sub>34</sub>O<sub>2</sub>Si

Synonyms:C₂₁H₃₄O₂Si

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Chemical Property of C₂₁H₃₄O₂Si

Chemical Property:

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Technology Process of C₂₁H₃₄O₂Si

There total 6 articles about C₂₁H₃₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415231-59-2
C₁₉H₃₀O₂Si

: 75-03-6
ethyl iodide

: 1415231-57-0
C₂₁H₃₄O₂Si

Guidance literature:: C₁₉H₃₀O₂Si; With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.666667h;

ethyl iodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 1h;
DOI:10.1016/j.tetlet.2012.07.010

Reference yield:

: 1395300-07-8
C₁₃H₁₆O₂

: 1415231-57-0
C₂₁H₃₄O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C

2.2: 1 h / -78 °C

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/j.tetlet.2012.07.010

Reference yield:

: 1415231-63-8
C₁₃H₁₄O₂

: 1415231-57-0
C₂₁H₃₄O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / ethanol / 0 - 20 °C

2.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C

3.2: 1 h / -78 °C

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.07.010