4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide

Base Information

Chemical Name:4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide
CAS No.:1433955-29-3
Molecular Formula:C₃₈H₃₀FNO
Molecular Weight:535.661
Hs Code.:

Synonyms:4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide

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Chemical Property of 4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide

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Technology Process of 4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide

There total 2 articles about 4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 70001-45-5
4-fluoro-N-isopropylbenzamide

: 501-65-5
diphenyl acetylene

: 1433955-29-3
4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 12h; under 760.051 Torr; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201200372

Reference yield:

: 403-43-0
4-fluorobenzoyl chloride

: 1433955-29-3
4-fluoro-N-isopropyl-5,6,7,8-tetraphenyl-1-naphthamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / 20 °C / Cooling with ice; Schlenk technique; Inert atmosphere

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate / N,N-dimethyl-formamide / 12 h / 100 °C / 760.05 Torr / Schlenk technique; Inert atmosphere

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201200372