6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

Base Information

Chemical Name:6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide
CAS No.:1334525-51-7
Molecular Formula:C₁₉H₁₅BrNO*I
Molecular Weight:480.143
Hs Code.:

Synonyms:6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

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Chemical Property of 6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

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Technology Process of 6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

There total 3 articles about 6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 131452-74-9
(2E)-1-(4-bromophenyl)-3-(6-quinolinyl)-2-propen-1-one

: 74-88-4
methyl iodide

: 1334525-51-7
6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

Guidance literature:: In acetone; for 10h; Reflux;
DOI:10.1016/j.ejmech.2011.07.019

Reference yield:

: 91-62-3
6-methylquinoline

: 1334525-51-7
6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: selenium(IV) oxide / 24 h / 150 - 160 °C

2: sodium hydroxide / ethanol / 0 - 20 °C

3: acetone / 10 h / Reflux

With selenium(IV) oxide; sodium hydroxide; In ethanol; acetone;
DOI:10.1016/j.ejmech.2011.07.019

Reference yield:

: 4113-04-6
quinoline-6-carbaldehyde

: 1334525-51-7
6-[(1E)-3-(4-bromophenyl)-3-oxo-1-propen-1-yl]-1-methylquinolinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 0 - 20 °C

2: acetone / 10 h / Reflux

With sodium hydroxide; In ethanol; acetone;
DOI:10.1016/j.ejmech.2011.07.019