methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

Base Information

Chemical Name:methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate
CAS No.:1421333-20-1
Molecular Formula:C₃₃H₃₅NO₄
Molecular Weight:509.645
Hs Code.:

Synonyms:methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

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Chemical Property of methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

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Technology Process of methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

There total 3 articles about methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₈H₄₅NO₆

: 1421333-20-1
methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

Guidance literature:: With dimethyl amine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

: 1380445-03-3
4-(((1S,2S)-2,3-dihydro-1-hydroxy-2-(1H-inden-2-yl)-1H-inden-2-yl)methyl)benzoic acid

: 1421333-20-1
methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2: dicyclohexyl-carbodiimide; dmap / ethyl acetate / 12 h / 20 °C

3: dimethyl amine / tetrahydrofuran / 1 h / 0 - 20 °C

With dmap; potassium carbonate; dimethyl amine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 35661-60-0
Fmoc-Leu-OH

: 1421332-97-9
methyl 4-(((1S,2S)-1-hydroxy-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

: 1421333-20-1
methyl 4-(((1S,2S)-1-(((S)-2-amino-4-methylpentanoyl)oxy)-2,3-dihydro-1H,1'H-[2,2'-biinden]-2-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / ethyl acetate / 12 h / 20 °C

2: dimethyl amine / tetrahydrofuran / 1 h / 0 - 20 °C

With dmap; dimethyl amine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;