C₂₃H₂₅ClO₆S

Base Information

Chemical Name:C₂₃H₂₅ClO₆S
CAS No.:1193783-66-2
Molecular Formula:C₂₃H₂₅ClO₆S
Molecular Weight:464.967
Hs Code.:

C<sub>23</sub>H<sub>25</sub>ClO<sub>6</sub>S

Synonyms:C₂₃H₂₅ClO₆S

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Chemical Property of C₂₃H₂₅ClO₆S

Chemical Property:

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Technology Process of C₂₃H₂₅ClO₆S

There total 10 articles about C₂₃H₂₅ClO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-{3-[(1S,5S)-5-(3-Chloro-5-hydroxymethyl-phenoxymethyl)-4-oxo-cyclopent-2-enyl]-propyl}-thiophene-2-carboxylic acid

: 107-21-1
ethylene glycol

: 1193783-66-2
C₂₃H₂₅ClO₆S

Guidance literature:: 5-{3-[(1S,5S)-5-(3-Chloro-5-hydroxymethyl-phenoxymethyl)-4-oxo-cyclopent-2-enyl]-propyl}-thiophene-2-carboxylic acid; With chloroformic acid ethyl ester; triethylamine; In dichloromethane; at 20 ℃; for 2.5h;

ethylene glycol; With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 58707-52-1
(3aR,4S,5R,6aS)-4-({[dimethyl(2-methyl-2-propanyl)silyl]oxy}methyl)-5-(tetrahydro-2H-pyran-2-yloxy)hexahydro-2H-cyclopenta[b]furan-2-ol

: 1193783-66-2
C₂₃H₂₅ClO₆S

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 6 h

3.1: triethylamine / dichloromethane / 0 - 20 °C

4.1: tetrabutyl-ammonium chloride / toluene / 18 h / 40 °C

5.1: tetrabutyl ammonium fluoride; water / tetrahydrofuran / 18 h / 20 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C

7.1: methanol / pyridinium p-toluenesulfonate / 20 - 40 °C

8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

9.1: Rabbit liver esterase / Rabbit liver esterase / acetonitrile / 24.17 h / 20 °C / pH 7.2

10.1: chloroformic acid ethyl ester; triethylamine / dichloromethane / 2.5 h / 20 °C

10.2: 20 °C

With methanol; Rabbit liver esterase; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; water; hydrogen; chloroformic acid ethyl ester; potassium carbonate; Dess-Martin periodane; triethylamine; triphenylphosphine; Rabbit liver esterase; palladium 10% on activated carbon; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 6.1: Mitsunobu reaction;

Reference yield:

: 960136-12-3
C₂₆H₄₄O₆SSi

: 1193783-66-2
C₂₃H₂₅ClO₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C

2.1: tetrabutyl-ammonium chloride / toluene / 18 h / 40 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C

4.1: methanol / pyridinium p-toluenesulfonate / 20 - 40 °C

5.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

6.1: Rabbit liver esterase / Rabbit liver esterase / acetonitrile / 24.17 h / 20 °C / pH 7.2

7.1: chloroformic acid ethyl ester; triethylamine / dichloromethane / 2.5 h / 20 °C

7.2: 20 °C

With methanol; Rabbit liver esterase; di-isopropyl azodicarboxylate; tetrabutyl-ammonium chloride; chloroformic acid ethyl ester; Dess-Martin periodane; triethylamine; triphenylphosphine; Rabbit liver esterase; pyridinium p-toluenesulfonate; In dichloromethane; toluene; acetonitrile; 3.1: Mitsunobu reaction;