3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

Base Information

Chemical Name:3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester
CAS No.:1402345-17-8
Molecular Formula:C₂₆H₂₄N₂O₇
Molecular Weight:476.486
Hs Code.:

Synonyms:3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

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Chemical Property of 3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

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Technology Process of 3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

There total 9 articles about 3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5781-53-3
monomethyl oxalyl chloride

: 1402345-16-7
3-methoxy-4-[3-oxo-3-(2-phenylamino-pyridin-3-yl)-propyl]-benzoic acid methyl ester

: 1402345-17-8
3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

Guidance literature:: In toluene; at 130 ℃; for 4h;

Reference yield:

: 619-12-5
4-formyl-3-hydroxybenzoic acid

: 1402345-17-8
3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 4 h / 25 °C

2: sodium methylate / methanol / 48 h / 25 °C

3: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; acetone

4: toluene / 4 h / 130 °C

With hydrogen; sodium methylate; potassium carbonate; palladium 10% on activated carbon; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; acetone; toluene; 2: Aldol Condensation;

Reference yield:

: 55676-21-6
3-acetyl-2-chloropyridine

: 1402345-17-8
3-methoxy-4-{3-[2-(methoxyoxalyl-phenyl-amino)-pyridin-3-yl]-3-oxo-propyl}-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: DL-10-camphorsulfonic acid / 1,4-dioxane / 3 h / 75 - 80 °C / Sealed tube

2: sodium methylate / methanol / 48 h / 25 °C

3: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; acetone

4: toluene / 4 h / 130 °C

With hydrogen; sodium methylate; palladium 10% on activated carbon; DL-10-camphorsulfonic acid; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate; acetone; toluene; 2: Aldol Condensation;