6-hydroxyhexyl phenyl carbonate

Base Information

• Chemical Name: 6-hydroxyhexyl phenyl carbonate
• CAS No.: 35652-55-2
• Molecular Formula: C₁₃H₁₈O₄
• Molecular Weight: 238.284
• Mol file: 35652-55-2.mol

Synonyms:6-hydroxyhexyl phenyl carbonate

Chemical Property of 6-hydroxyhexyl phenyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 6-hydroxyhexyl phenyl carbonate

There total 2 articles about 6-hydroxyhexyl phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1,6-hexanediol (629-11-8) + phenyl chloroformate (1885-14-9) → 6-hydroxyhexyl phenyl carbonate (35652-55-2)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 18.5h;

DOI:10.1002/ejoc.200900241

Reference yield:

bis(phenyl) carbonate (102-09-0) + 1,6-hexanediol (629-11-8) → 6-hydroxyhexyl phenyl carbonate (35652-55-2)

Guidance literature:

With Yb(1,3,5-benzenetricarboxylate); at 180 ℃; for 3h; Inert atmosphere;

DOI:10.1007/s13738-020-01929-8

Reference yield: 41.0%

(3R,4R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-3,4-diaminopyrrolidine + 6-hydroxyhexyl phenyl carbonate (35652-55-2) → C41H63N3O5

Guidance literature:

With pyridine; Reflux;

DOI:10.1002/ejoc.200900241

upstream raw materials:

1,6-hexanediol

phenyl chloroformate

bis(phenyl) carbonate