(E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid

Base Information

Chemical Name:(E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid
CAS No.:952282-39-2
Molecular Formula:C₂₃H₂₃ClN₂O₃
Molecular Weight:410.9
Hs Code.:

Synonyms:(E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid

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Chemical Property of (E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid

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Technology Process of (E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid

There total 1 articles about (E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952281-99-1
1-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-ethanone

: 66885-68-5
(E)-p-formylcinnamic acid

: 952282-39-2
(E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid

Guidance literature:: 1-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-ethanone; (E)-p-formylcinnamic acid; With potassium hydroxide; ethanol; at 0 ℃; for 6h;

With hydrogenchloride; In ethanol; water; pH=6;

Reference yield:

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 952282-39-2
(E)-3-(4-{(E)-3-[2-chloro-5-(4-methyl-piperazin-1-yl)-phenyl]-3-oxo-propenyl}-phenyl)-acrylic acid

: C₂₈H₃₂ClN₃O₄

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;