(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

Base Information

Chemical Name:(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene
CAS No.:335004-51-8
Molecular Formula:C₃₉H₅₁N₃O₁₀S₃
Molecular Weight:818.046
Hs Code.:

Synonyms:(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

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Chemical Property of (E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

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Technology Process of (E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

There total 4 articles about (E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 70-55-3
toluene-4-sulfonamide

: 335004-44-9
N-[(E)-4-bromo-2-butenyl]-N-(tert-butyloxycarbonyl)-(4-methylphenyl)sulfonamide

: 335004-51-8
(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

Guidance literature:: With potassium carbonate; In acetonitrile; for 20h; Heating;
DOI:10.1002/1099-0690(200101)2001:2<329::aid-ejoc329>3.0.co;2-n

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 335004-51-8
(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Et₃N; DMAP / CH₂Cl₂

2: 95 percent / K₂CO₃ / acetonitrile / 5 h / Heating

3: 96 percent / K₂CO₃ / acetonitrile / 20 h / Heating

With dmap; potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/1099-0690(200101)2001:2<329::aid-ejoc329>3.0.co;2-n

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 335004-51-8
(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / acetonitrile / 5 h / Heating

2: 96 percent / K₂CO₃ / acetonitrile / 20 h / Heating

With potassium carbonate; In acetonitrile;
DOI:10.1002/1099-0690(200101)2001:2<329::aid-ejoc329>3.0.co;2-n