(2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

Base Information

Chemical Name:(2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene
CAS No.:909801-46-3
Molecular Formula:C₃₃H₃₆F₃NO₄
Molecular Weight:567.648
Hs Code.:

Synonyms:(2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

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Chemical Property of (2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

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Technology Process of (2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

There total 3 articles about (2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 909801-45-2
(2R,3R,4R)-1,3,4-Tris(benzyloxy)-N-(but-3-en-1-yl)hex-5-en-2-amine

: 407-25-0
trifluoroacetic anhydride

: 909801-46-3
(2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1039/b605818c

Reference yield:

: methyl 1,3,4-tri-O-benzyl-6-deoxy-6-iodo-D-fructofuranoside

: 909801-46-3
(2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / zinc / H₂O; tetrahydrofuran / 2 h / 40 °C / sonication

2: 3 Angstroem molecular sieves; InCl₃; NaCNBH₃ / tetrahydrofuran / 3 h / 20 °C

3: 82 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With indium(III) chloride; 3 A molecular sieve; sodium cyanoborohydride; triethylamine; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/b605818c

Reference yield:

: 220939-94-6
(3S,4R)-1,3,4-tris(benzyloxy)-hex-5-en-2-one

: 909801-46-3
(2R,3R,4R)-N-trifluoroacetyl-1,3,4-tris(benzyloxy)-2-(but-3-enylamino)-hex-5-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 3 Angstroem molecular sieves; InCl₃; NaCNBH₃ / tetrahydrofuran / 3 h / 20 °C

2: 82 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With indium(III) chloride; 3 A molecular sieve; sodium cyanoborohydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b605818c