methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

Base Information

Chemical Name:methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate
CAS No.:1033591-50-2
Molecular Formula:C₂₂H₃₅BrO₇
Molecular Weight:491.42
Hs Code.:

Synonyms:methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

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Chemical Property of methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

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Technology Process of methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

There total 2 articles about methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1033591-49-9
methyl (2S,3S,5R)-6-(3-bromo-2-hydroxy-5-isopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

: 75-26-3
isopropyl bromide

: 1033591-50-2
methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1021/ol800749w

Reference yield: 72.0%

: 1033591-48-8
methyl (2S,3S,5S,6S)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-3-methoxy-5-methyltetrahydro-2H-pyran-2-carboxylate

: 1033591-49-9
methyl (2S,3S,5R)-6-(3-bromo-2-hydroxy-5-isopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

: 1033591-50-2
methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

Guidance literature:: methyl (2S,3S,5S,6S)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-3-methoxy-5-methyltetrahydro-2H-pyran-2-carboxylate; With triethylsilane; scandium tris(trifluoromethanesulfonate); In dichloromethane; for 20h; Inert atmosphere;

With water; In dichloromethane; for 0.166667h; Inert atmosphere;
DOI:10.1021/ol800749w

Reference yield: 98.0%

: 1033591-50-2
methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate

: 1033591-55-7
(2R,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-3-methoxy-5-methylhexane-1,2-diol

Guidance literature:: methyl (2S,3S,5R)-6-(3-bromo-2,5-diisopropoxy-6-methoxyphenyl)-2-hydroxy-3-methoxy-5-methylhexanoate; With methanol; lithium borohydride; In diethyl ether; at 0 - 20 ℃; for 6h; Inert atmosphere;

With hydrogenchloride; water; In diethyl ether; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ol800749w